Crystal field states in a Quantum Spin Ice]{Crystal field states of Pr$^{3+}$ in the candidate quantum spin ice Pr$_{2}$Sn$_{2}$O$_{7}$

(2013)

Authors:

AJ Princep, D Prabhakaran, AT Boothroyd, DT Adroja

Spin fluctuations away from (pi,0) in the superconducting phase of molecular-intercalated FeSe

(2013)

Authors:

AE Taylor, SJ Sedlmaier, SJ Cassidy, EA Goremychkin, RA Ewings, TG Perring, SJ Clarke, AT Boothroyd

Ball-milling-induced amorphization of zeolitic imidazolate frameworks (ZIFs) for the irreversible trapping of iodine.

Chemistry (Weinheim an der Bergstrasse, Germany) 19:22 (2013) 7049-7055

Authors:

Thomas D Bennett, Paul J Saines, David A Keen, Jin-Chong Tan, Anthony K Cheetham

Abstract:

The I2-sorption and -retention properties of several existing zeolitic imidazolate frameworks (ZIF-4, -8, -69) and a novel framework, ZIF-mnIm ([Zn(mnIm)2 ]; mnIm=4-methyl-5-nitroimidazolate), have been characterised using microanalysis, thermogravimetric analysis and X-ray diffraction. The topologically identical ZIF-8 ([Zn(mIm)2]; mIm=2-methylimidazolate) and ZIF-mnIm display similar sorption abilities, though strikingly different guest-retention behaviour upon heating. We discover that this guest retention is greatly enhanced upon facile amorphisation by ball milling, particularly in the case of ZIF-mnIm, for which I2 loss is retarded by as much as 200 °C. It is anticipated that this general approach should be applicable to the wide range of available metal-organic framework-type materials for the permanent storage of harmful guest species.

Aminoff Prize in crystallography

Physica Scripta IOP Publishing 87:4 (2013) 048101

Absence of strong magnetic fluctuations in the iron phosphide superconductors LaFePO and Sr2ScO3FeP

(2013)

Authors:

AE Taylor, RA Ewings, TG Perring, DR Parker, J Ollivier, SJ Clarke, AT Boothroyd